Institute of Fundamental Technological Research
Polish Academy of Sciences

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F. Zupanič


Recent publications
1.  Jelen Z., Krajewski M., Zupanič F., Majerič P., Švarc T., Anžel I., Ekar J., Liou S., Kubacki J., Tokarczyk M., Rudolf R., Melting point of dried gold nanoparticles prepared with ultrasonic spray pyrolysis and lyophilisation, nanotechnology reviews, ISSN: 2191-9097, DOI: 10.1515/ntrev-2022-0568, Vol.12, No.1, pp.1-12, 2023

Abstract:
A coupled process of ultrasonic spray pyrolysis and lyophilisation was used for the synthesis of dried gold nanoparticles. Two methods were applied for determining their melting temperature: uniaxial microcompression and differential scanning calorimetry (DSC) analysis. Uniaxial microcompression resulted in sintering of the dried gold nanoparticles at room temperature with an activation energy of 26–32.5 J/g, which made it impossible to evaluate their melting point. Using DSC, the melting point of the dried gold nanoparticles was measured to be around 1064.3°C, which is close to pure gold. The reason for the absence of a melting point depression in dried gold nanoparticles was their exothermic sintering between 712 and 908.1°C.

Keywords:
gold nanoparticles, melting point, ultrasonic spray pyrolysis, characterisation

Affiliations:
Jelen Z. - other affiliation
Krajewski M. - IPPT PAN
Zupanič F. - other affiliation
Majerič P. - other affiliation
Švarc T. - other affiliation
Anžel I. - other affiliation
Ekar J. - other affiliation
Liou S. - University of Maryland (US)
Kubacki J. - Silesian University of Technology (PL)
Tokarczyk M. - University of Warsaw (PL)
Rudolf R. - other affiliation

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